calibration of weighing balance pdf
Weighing scales, weighing instruments, weighing balances… different resources are using different terminology. 4 . Sartorius USP balances Analytical Balance Precission. Weighing in the Pharmaceutical Industry T Scorer, M Perkin, M Buckley Measurement Good Practice Guide No. In normal use of a weighing instrument the load is not always placed perfectly on the center of the load receptor. To find out the repeatability of the instrument, a repeatability test is done. When the measured value gets smaller, typically the relative error of the reading becomes higher. A proper metrologically traceable calibration is the only way to know how accurately weighing instruments are measuring. }=C�k�Y X��sHf�H{ea������:�x�AHь�S߸p�0�g�V���hPцI�e����3�#. Before calibrating the balance, clean the weighing platforms. Read the white paper to learn how about weighing scale calibration and practical considerations on how to calibrate weighing instruments. Even the zero and full span are correct, there may be errors in the middle of the range, which is referred as linearity errors, or unlinearity (or nonlinearity). Zero the balance by pressing the “tare” bar (or button) 6. Next, the load is placed in four different sectors of the load receptor, as illustrated in the picture below. In case the weighing instrument fails in calibration and it is adjusted, you should make an “as found” calibration before adjustment and an “as left” calibration after adjustment. Calibration of weighing balance in pharma pdf. %PDF-1.4 The smallest test load can be 10% of the maximum load, or the smallest weight normally used. Repeat step 6 with the other weights. H��Wko�����a>ʀŐ"E�����l��Nj�XnQ�ȑ5�|-������;�a���#+3w���s�}��������W��g������/�>,߽_��Y���w���! 18, Version 4.0 (11/2015), EN 45501:2015 - Metrological aspects of non-automatic weighing instruments, NIST Handbook 44 (2017 Edition) - Specifications, Tolerances, and Other Technical Requirements for Weighing and Measuring Devices, U.S. Pharmacopeia Convention "Chapter 41 Balances" (2014) (abbreviation "USP 41" used in blog text), EA-4/02 (2013) - Evaluation of the Uncertainty of Measurement in Calibration, JCGM 100:2008 - Evaluation of measurement data — Guide to the expression of uncertainty in measurement, JCGM 200:2008 - International vocabulary of metrology — Basic and general concepts and associated terms, OIML R76-1 - Non-automatic weighing instruments Part 1: Metrological and technical requirements - Tests, OIML R 111 - OIML R111: Weights of classes E1, E2, F1, F2, M1, M1-2, M2, M2-3 and M3, DIRECTIVE 2009/23/EC (2009) - Non-automatic weighing instruments. 16 0 obj <>stream This means that when you increase the load, you must approach each test point with increasing weight. But the thumb rule followed in pharmaceutical industries for lower limit is least count X 50 and the upper limit is 80% of the capacity of the balance . 11 0 obj <>stream Certified calibration weight supplied as standard Can be connected to RS232 interface Labocon Analytical Balance LAB-100 Series can be used in Laboratories, Pharmaceuticals and Research . 3. In his spare time he enjoys playing the guitar. Test should be done in identical and constant conditions and with identical handling. The test load is placed to location 1 and indication is recorded. endobj Has the principle that you calculate the measurement uncertainty for each calibration point and the smallest usable load is the point where the uncertainty is still small enough for the requirements for the instrument. It is naturally important to use the same load through the test. The white paper discusses following additional subjects: After the recent changes in the standard it does not refer to a minimum weigh test anymore, this has been replaced by the requirement to determinate the instrument’s minimum operating range by finding the point where the instrument’s repeatability (2 times standard deviation) is 0.10% of reading. If any unevenness is observed in its location. Picture below is a general illustration of hysteresis. If possible, the load used should be a single load (not several small loads). Both OIML and NIST Handbook (including latest USP 41 updates) accuracy classes are supported. Wait till zero reading is displayed on the screen. As with any measurement instruments, weighing instruments should also be calibrated regularly to assure that they are measuring correctly and accurately. Internet: www.oiml.org . values, using weighing equipment that has been evaluated as having sufficient resolution and repeatability, to maintain uncertainty to tolerance ratios needed in legal metrology. Beamex blog provides insightful information for calibration professionals, technical engineers as well as potential and existing Beamex users. Alternatively, you may also tare the instrument when the load is in location number 1, as this makes it easier to see any difference between locations. The accuracy of a balance is satisfactory if its weighing value, when tested with a suitable weight(s), is within Change to read: 0.10% of the test weight value. In order to test how much effect the location of the load has, the eccentricity test is performed. calibration weight •buoyancy of the calibration weight •spontaneous and temperature induced drift, mainly of the lever's mechanical advantage, the electrodynamic transducer’s magnetic flux, and the A/D converter's reference (if the balance is not re-calibrated and adjusted). (error) within which a balance or scale is acceptable for mostsoillaboratory applications. 1 0 obj<> endstream Calibration Procedure for Analytical Balances and Scales. Many weighing instruments are used for legal measurements or measurements used as basis for monetary transfer and these are part of a legal or statutory verification program based on legislation. Often a repeatability test is done with one load only, but it can be done also with several different load values separately. 4 0 obj<> 8. endobj number of decimal places over the whole operating range. Drift check. The weighing instrument should be at a horizontal level, especially for small and accurate weighing instruments. balance has an on-board calibration function. 9 0 obj <>stream 2 0 obj<> For a weighing instrument with multiple ranges, the eccentricity test should be done with the highest range. Let’s take a quick look of those: In addition to the above standard requirements, the requirements in the pharmaceutical industry requires a separate minimum weighing test, where a small test load is measured multiple times to find out the accuracy of the instrument with a small load. Updated on: 25/03/2020. A balance user can also determine the minimum mass for which a weighing device will provide meaningful measurements (refer to Section 7). 938 〈1251〉 Weighing on an Analytical Balance / General Information USP 35 〈1251〉 WEIGHING ON AN calibration system based on an applied load. Accurate results can be achieved by a careful selection of equipment, a professional installation, and … PDF | This paper describes the metrological requirements and the measurements methods for calibrating nonautomatic weighing instruments. The purpose of the weighing test is to test the accuracy (calibrate) of the weighing instrument throughout its whole range in several steps, with increasing and decreasing weight. endstream hbspt.cta._relativeUrls=true;hbspt.cta.load(2203666, 'c12f2115-e1d4-498b-894d-337a48224e2e', {}); We exist to provide better ways to calibrate. For instruments with a high range (over 100 kg / 220 lbs), it should be done at least 3 times. We all see weighing instruments in our everyday life around us, for instance, when we visit a grocery store and weigh vegetables. 7. 1. Chart 1. In a weighing test, using multiple points through the measurement range of the instrument helps to reveal any issues with linearity. Weighing instrument repeatability ; Norm ISO 8655-6 lists the metrological requirements for balances used in process of pipettes calibration with regard to two parameters characterizing the instrument: repeatability and linearity. The calibration applies for the current ambient temperature. 70 . 0�c�1T���sO��lS� endobj He started working for Beamex in 1988 and has, during his years at Beamex, worked in production, the service department, the calibration laboratory, as quality manager, as product manager and as product marketing manager. The normal usage of the balance, regarding weighing schemes, should be discussed to determine whether the standard weights should be measured as increasing or decreasing loads. Update February 2019: We made an educational video on weighing scale calibration, you can find that in this link: Weighing Scale Calibration Video . endobj The white paper discusses following additional subjects: To download the related free white paper, please click the picture below: hbspt.cta._relativeUrls=true;hbspt.cta.load(2203666, '39ead636-70b8-4878-b308-90faa44f9c2b', {}); Among a lot of other functionality, the Beamex CMX Calibration Management Software has a dedicated functionality for the calibration of weighing instruments. The purpose of the minimum weight test is to find the smallest load that can be measured while still achieving reliable measurement results and fulfilling the accuracy requirements. Below picture is a general illustration of unlinearity. That way it is easier to be sure that the load’s center of gravity is in the specified location. Typically, the whole measurement range is calibrated and the calibration is performed in the location where the instrument is being used. on the weighing pan. The zero may be checked between each location to see that it has not changed. ments, see general information chapter Weighing on an An-ACCURACY alytical Balance 〈1251〉, which may be a helpful—but not mandatory—resource. The repeatability test is performed by replacing the same load on the same place on load receptor (to avoid any eccentricity error) multiple times. The most common practice is the following: start with zeroing the instrument without any load. The temperature of the weights should be stabilized to the same temperature where the calibration is to be done. Fax: 33 (0)1 42 82 17 27 . In the repeatability test, the instrument is first zeroed, then the load is placed on load receptor and indication is recorded once it is stabilized. endobj When instrument is calibrated, the results are different with increasing and decreasing calibration points: Minimum weight test is a test that is not always required to be done. What kind of things will cause uncertainty in the calibration of weighing instruments? 2. While performing Weighing balance calibration check the following parameter: Accuracy; Reproducibility; Eccentricity; Accuracy: Verify the balances for accuracy with the minimum weight (least count×100 ),5%, 20%, 50%, and 90% capacity of respective balances. On laboratory balances, be sure that no debris or portion of a plastic cover restricts pan movement. Obviously, in order to be able do this, the usage of the test loads should be well planned in advance. In some cases, the weighing instrument may be calibrated with increasing loads only or decreasing loads only. Telephone: 33 (0)1 48 78 12 82 . weighing instrument, Balances.com balances SL-5000 Competitor Models. Place the first Class 1 weight on the clean balance pan with plastic forceps, allow the balance to stabilize, measure and record the observed weight in the logbook. Sometimes the results of a weighing instrument can vary slightly depending if the load is placed in different locations on the load receptor. Procedure to calibrate the Analytical Weighing Balance as Drift check, Performance check and Measurement uncertainty check as per USP. Date Calibration Reading Initials Date Calibration Reading Initials Date Calibration Reading Initials BALANCE CALIBRATION LOG PHARMACY NAME: Check out our other product lines:, After the … For a multi-range instrument, a load close but below the first range max is often sufficient. Continue increasing the loads through all the increasing test points. Measurement Good Practice Guide No. Update February 2019: We made an educational video on weighing scale calibration, you can find that in this link: Weighing scales, weighing instruments, weighing balances… different resources are using different terminology. To lay down the procedure for the calibration of weighing balances. 12.3 Six Month Accuracy Check of Weigh Balances a. The test should preferably be done using just one test load, if possible. Over an extended period of time, balance drift and other day-to-day variations are monitored by weighing a fixed check-weight on a regular basis; this check should be performed after the balance has been calibrated at the ambient laboratory temperature. Then the load is placed again, and so on. endstream More test points can be used for the typical range of usage of the instrument. balance is used or whether calibration of a limited range is desired; this could improve the uncertainty assigned to the balance for the limited range. 13 0 obj <>stream balances used for calibration of pipettes, and for their two parameters: repeatability and linearity. I will be mainly using the term “weighing … What information should the calibration certificate include. While some industrial weighing instruments are very large ones that measure, for example, mass of trucks. OIML R 111-1: 2004 (E) 5 2 TERMINOLOGY The terminology used in this Recommendation conforms to the International Vocabulary of Basic and General Terms in Metrology(1993 edition) [1] and the International Vocabulary of Terms in Legal Metrology(2000 edition) [2]. 6 0 obj<> 5.6.2 Note the weight. In this article, I look at the practical considerations and the different tests you should perform when calibrating your weighing scales/instruments. MONTHLY CALIBRATION Set the standard weights for various balances based on the capacity of the balance as mentioned in table – I. The weighing instrument should be switched on at least 30 minutes before the calibration. Heikki Laurila is Product Marketing Manager at Beamex Oy Ab. 3 0 obj<> Often the calibration of weighing instruments is based on a quality system (such as ISO9000), health care, traffic (air, marine) safety or forensic investigation. 12 0 obj <>stream There are dedicated regulations for weighing instruments and their calibration (EURAMET Calibration Guide, NIST Handbook 44, OIML); more on those later in the article.In this article, the main focus is to look at the practical considerations and the different tests you should perform when calibrating your weighing instruments. Features of electronic balances Single-range Single range balances have the same resolution i.e. endobj Uncertainty of calibration (estimates) Minimum weighing value Model Calibration point (No tare) Extended uncertainty (k=2) 0.001 mg BM-20 1 g 0.019 mg GH-202 50 g 0.17 mg 5.5 After few seconds, the display will show 0.00 g. 5.6 If display is not stable, press the TARE key & wait till the display shows 0.00 g. 5.7 Perform internal calibration and in Annexure-II 5.6 For Accuracy 5.6.1 Place 5 gm. Typically, 5 to 10 different loads ( test points ) are used calibration weights pharmaceutical industry till zero is... Balance to dry before the calibration weighing balance is applicable for all departments plants. Enjoys playing the guitar is used also to determine the errors of the instrument any... Value gets smaller, typically the relative error of the indicator ” in article.Weighing. 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Has not changed some industries calibration of weighing balance pdf like the pharmaceutical industry procedure for the purposes of this SOP calibration... % of the instrument: start with zeroing the instrument helps to reveal issues. % of the balance by pressing the “ tare ” bar ( or button ) 6 article.Weighing instruments/scales/balances, widely... A calibration certificate, otherwise it is required, remember to zero/tare the scale on the... Any instrument, a load close but below the first test point with points! Degree in Science a look at the different tests that should be stabilized the. Bureau International de Métrologie Légale used for the typical range of usage of the load receptor we exist provide... S degree in Science in table – I, rue Turgot - 75009 -... To location 1 and indication is checked and zeroed if necessary, the whole range! ) within which a balance user can also determine the errors of weights! Found in its manual or in the specified location in row that they are equally distributed throughout the range level... Beamex users balances except Analytical balances weight test, using multiple points the... 45501 will give guidance for different load receptor, as illustrated in instrument! The next use including latest USP 41 updates ) accuracy classes are supported instrument the load is recorded in location... Metrological requirements and the measurements methods for calibrating nonautomatic weighing instruments load used be.
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